1.1: tert.-butyl lithium / tetrahydrofuran / 2 h / -78 °C
1.2: -78 - 20 °C
2.1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile; bromine / benzene / 24 h / Reflux
View Scheme
参考文献
Motto, John M.; Castillo, Alvaro; Greer, Alexander; Montemayer, Laura K.; Sheepwash, Erin E.; Schwan, Adrian L.
Tetrahedron, 2011 , vol. 67, # 5 p. 1002 - 1010