1-甲氧基-4-[(1E)-2-硝基-1-丙烯-1-基]苯合成路线 （共 22 条）
反应条件
1: With lithium aluminium tetrahydride in diethyl ether Reduction; 2 h; Heating; 2: With Candida antarctica lipase B; ethyl acetate; triethylamine T=30°C; racemate resolution; 4 h; Title compound not separated from byproducts;
参考文献
Campos, Francisco; Bosch, M. Pilar; Guerrero, Angel
Tetrahedron Asymmetry, 2000 , vol. 11, # 13 p. 2705 - 2717
反应条件
1: 78 percent / LiAlH4 / diethyl ether / 2 h / Heating 2: Candida antarctica lipase B 3: 3M aq. KOH / Heating View Scheme
参考文献
Campos, Francisco; Bosch, M. Pilar; Guerrero, Angel
Tetrahedron Asymmetry, 2000 , vol. 11, # 13 p. 2705 - 2717
反应条件
1: ethanol; acetic acid; aqueous sulfuric acid / bei der elektrochemischen Reduktion 2: aqueous hydrochloric acid View Scheme
参考文献
Alles
Journal of the American Chemical Society, 1932 , vol. 54, p. 271,273
反应条件
trifluoroacetic acid; zinc in N,N-dimethyl-formamide 0.25 h;
参考文献
Saikia, Anil K.; Barua, Nabin C.; Sharma, Ram P.; Ghosh, Anil C.
Journal of Chemical Research - Part S, 1996 , # 2 p. 124 - 125
参考文献
Hoover; Hass
Journal of Organic Chemistry, 1947 , vol. 12, p. 501,504
反应条件
MCM-41-NH2
T=90°C; 6 h;
参考文献
Demicheli, Giuseppina; Maggi, Raimondo; Mazzacani, Alessandro; Righi, Paolo; Sartori, Giovanni; Bigi, Franca
Tetrahedron Letters, 2001 , vol. 42, # 12 p. 2401 - 2403
反应条件
triethylamine; triphenylphosphine in tetrachloromethane
2 h; Heating;
参考文献
Saikia; Barua; Sharma; Ghosh
Synthesis, 1994 , # 7 p. 685 - 686
反应条件
2,2'-azo-bisisobutyronitrile; nitric acid in acetonitrile
T=50°C; nitro-Hunsdiecker reaction; 9 h;
参考文献
Das, Jaya Prakash; Sinha, Pradipta; Roy, Sujit
Organic Letters, 2002 , vol. 4, # 18 p. 3055 - 3058
反应条件
(E,Z)-crotononitrile; ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride; piperidinium acetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene
8 h; Inert atmosphereReflux;
参考文献
Hall, Michael I.; Pridmore, Simon J.; Williams, Jonathan M. J.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 1975 - 1978
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in toluene
T=150°C; Wadsworth-Emmons reaction; 72 h;
参考文献
Black, Phillip. J.; Cami-Kobeci, Gerta; Edwards, Michael G.; Slatford, Paul A.; Whittlesey, Michael K.; Williams, Jonathan M. J.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 1 p. 116 - 125
