2,2,3,3,4,4-六氟环-1,5-戊二醇合成路线 （共 6 条）
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Dobina,Kh.A. et al.
J. Appl. Chem. USSR (Engl. Transl.), 1973 , vol. 46, p. 687 - 689,732 - 734
反应条件
PPh3.Br2 in tetrachloromethane
参考文献
Matyushecheva,G.I. et al.
Journal of Organic Chemistry USSR (English Translation), 1971 , vol. 7, p. 1704 - 1706
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, p. 1641 - 1643
反应条件
1: aq. NaOH 2: NaI / bis-(2-hydroxy-ethyl) ether / 150 - 160 °C View Scheme
参考文献
Matyushecheva,G.I. et al.
Journal of Organic Chemistry USSR (English Translation), 1971 , vol. 7, p. 1704 - 1706
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, p. 1641 - 1643
反应条件
1: sulfuric acid / 250 °C 2: chlorine / unter Belichtung 3: antimony-dichloride-trifluoride / 160 °C View Scheme
参考文献
Henne; Richter
Journal of the American Chemical Society, 1952 , vol. 74, p. 5420
A.P.I.Res.Project, 1950 , vol. 44, # 1053
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in water
15 h; Ambient temperature;
参考文献
Serrurier, Cecile Bassilana; Cambon, Aime
Journal of Fluorine Chemistry, 1998 , vol. 87, # 1 p. 37 - 40
反应条件
1: ethanol; sodium ethylate; dioxane / Erhitzen des vom Aethanol befreiten Reaktionsgemisches mit Bromessigsaeure-aethylester
2: water; formic acid
View Scheme
参考文献
McBee et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 1721
