1H,1H,9H-十六氟-1-壬醇合成路线 (共 7 条)
反应条件
in benzene T=40°C; Abramov reaction; 10 h; Inert atmosphere;
参考文献
Krutikova; Krutikov; Erkin
Russian Journal of General Chemistry, 2010 , vol. 80, # 3 p. 428 - 433
反应条件
tert-butyl-octyl peroxide T=170°C;
参考文献
Industrial and Engineering Chemistry, , vol. 51, p. 829
US2559628 , ;
反应条件
potassium permanganate; acetic acid beim Erhitzen des Natrium-Salzes der erhaltenen Saeure in Aethylenglykol;
参考文献
Matsuo, Keizo; Stockmayer, Walter H.
Journal of Physical Chemistry, 1981 , vol. 85, # 22 p. 3307 - 3311
反应条件
sodium hydroxide; CuCl2
参考文献
Hoechst Aktiengesellschaft
Patent: US5495034 A1, 1996 ;
反应条件
potassium permanganate
参考文献
Matsuo, Keizo; Stockmayer, Walter H.
Journal of Physical Chemistry, 1981 , vol. 85, # 22 p. 3307 - 3311
反应条件
1: 77 percent / NaH, LiBr / diethyl ether / -20 °C 2: 60 percent / KMnO4 / acetic acid / Heating View Scheme
参考文献
Nguyen, T.; Rubinstein, M.; Wakselman, C.
Synthetic Communications, 1983 , vol. 13, # 1 p. 81 - 86
反应条件
potassium hydroxide in benzene
T=80°C; 1 h;
参考文献
Shilin, S. V.; Florensova, O. N.; Chernov, N. F.; Voronkov, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 8.2 p. 1838 - 1840,1697 - 1699