1-(2-溴乙基)-3,5-二甲氧基苯合成路线 （共 13 条）
反应条件
bromine; triphenylphosphine in dichloromethane
T=20°C; 48 h;
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Jamieson, Sally V.; Tuchinda Patoomratana; Whitaker, Alison J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1485 - 1492
反应条件
phosphorus tribromide
参考文献
Jamie, Joanne F.; Rickards, Rodney W.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 24 p. 3613 - 3621
反应条件
acetone; lithium bromide
参考文献
Heck; Winstein
Journal of the American Chemical Society, 1957 , vol. 79, p. 3114,3117
反应条件
1: ethanol
2: (i) NaOH, MeOH, (ii) /BRN= 102415/
3: LiAlH4
4: PBr3
View Scheme
参考文献
Bhati,A.
Tetrahedron, 1962 , vol. 18, p. 1519 - 1526
反应条件
1: (i) LiAlH4, (ii) PBr3
2: ethanol
3: (i) NaOH, MeOH, (ii) /BRN= 102415/
4: LiAlH4
5: PBr3
View Scheme
参考文献
Bhati,A.
Tetrahedron, 1962 , vol. 18, p. 1519 - 1526
反应条件
1: 100 percent / LiAlH4 / tetrahydrofuran / 2 h / 0 - 20 °C
2: 53 percent / PBr3
View Scheme
参考文献
Jamie, Joanne F.; Rickards, Rodney W.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 24 p. 3613 - 3621
反应条件
1: (i) NaOH, MeOH, (ii) /BRN= 102415/
2: LiAlH4
3: PBr3
View Scheme
参考文献
Bhati,A.
Tetrahedron, 1962 , vol. 18, p. 1519 - 1526
反应条件
1: LiAlH4
2: PBr3
View Scheme
参考文献
Bhati,A.
Tetrahedron, 1962 , vol. 18, p. 1519 - 1526
反应条件
1: Ag2O
2: LiAlH4
3: CCl4; PBr3
View Scheme
参考文献
Carnmalm
Acta Chemica Scandinavica (1947-1973), 1955 , vol. 9, p. 246,249
反应条件
1: LiAlH4
2: CCl4; PBr3
View Scheme
参考文献
Carnmalm
Acta Chemica Scandinavica (1947-1973), 1955 , vol. 9, p. 246,249
