苯基甲基3-甲基丁-2-烯酸酯合成路线 （共 15 条）
反应条件
1: (i) Zn, (ii) /BRN= 635680/
2: H2SO4 / benzene / Heating
View Scheme
参考文献
Taniguchi,M. et al.
Chemical and Pharmaceutical Bulletin, 1972 , vol. 20, p. 1438 - 1444
参考文献
Defensor
Patent: US2554947 , 1947 ;
参考文献
Majetich, George; Casares, Ada M.; Chapman, D.; Behnke, M.
Tetrahedron Letters, 1983 , vol. 24, # 18 p. 1909 - 1912
反应条件
chloro-trimethyl-silane in diethyl ether; dichloromethane
T=-78 - 0°C;
参考文献
Asao, Naoki; Lee, Sunyoung; Yamamoto, Yoshinori
Tetrahedron Letters, 2003 , vol. 44, # 22 p. 4265 - 4266
反应条件
AD-mix-α; methanesulfonamide; sodium hydrogencarbonate in water; tert-butyl alcohol
T=0°C; 60 h;
参考文献
Bryant, Helen J.; Dardonville, Christophe Y.; Hodgkinson, Timothy J.; Hursthouse, Michael B.; Malik, K. M. Abdul; Shipman, Michael
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 7 p. 1249 - 1255
