4-硝基-3-己烷基乙酸酯合成路线 （共 17 条）
反应条件
P(MeNCH2CH2)3N in tetrahydrofuran; isopropyl alcohol
T=-20 - -15°C; 2 h;
参考文献
Tang; Verkade
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7793 - 7802
反应条件
hydrogenchloride; 1,8-diazabicyclo[5.4.0]undec-7-ene in nitrogen
参考文献
CANON KABUSHIKI KAISHA; EHIME UNIVERSITY
Patent: US2008/171403 A1, 2008 ;
反应条件
in tetrahydrofuran; diethyl ether
参考文献
Iowa State University Research Foundation, Inc.
Patent: US5672717 A1, 1997 ;
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in various solvent(s)
T=20°C; Barton-Zard pyrrole synthesis; 2 h;
参考文献
Bhattacharya, Apurba; Cherukuri, Sankara; Plata, Robert Erik; Patel, Nitinchandra; Tamez Jr., Victoriano; Grosso, John A.; Peddicord, Michael; Palaniswamy, Venkatapuram A.
Tetrahedron Letters, 2006 , vol. 47, # 31 p. 5481 - 5484
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran; isopropyl alcohol
15 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tang; Verkade
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7793 - 7802
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran; isopropyl alcohol
15 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tang; Verkade
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7793 - 7802
反应条件
1: 81 percent / potassium carbonate / tetrahydrofuran; ethanol / 72 h / 20 °C
2: 88 percent / NaOH / ethanol; H2O / Heating
3: 68 percent / H2O / Heating
4: 80 percent / H2O2; pyridine / methanol / Heating
View Scheme
参考文献
Roth, Steven D.; Shkindel, Tetyana; Lightner, David A.
Tetrahedron, 2007 , vol. 63, # 45 p. 11030 - 11039
