全氟pentanal 水合物合成路线 (共 9 条)
反应条件
1: 59.6 percent / acetic acid / Heating 2: 98.3 percent / conc. H2SO4 View Scheme
参考文献
Latypov, R. R.; Belogai, V. D.; Pashkevich, K. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 1 p. 108 - 114
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 1 p. 123 - 128
反应条件
phosphorus pentoxide
T=60 - 70°C; Yield given;
参考文献
Hu, Chang-Ming; Chen, Jian
Journal of Fluorine Chemistry, 1994 , vol. 67, # 2 p. 189 - 192
反应条件
lead(II) bromide; aluminium
1.5 h; Ambient temperature;
参考文献
Hu, Chang-Ming; Tang, Xiao-Qing
Journal of Fluorine Chemistry, 1993 , vol. 61, # 3 p. 217 - 222
反应条件
1: lithium aluminium tetrahydride / diethyl ether / 0 °C
2: sulfuric acid; water / ethanol
View Scheme
参考文献
Cornut, Damien; Lemoine, Hugues; Kanishchev, Oleksandr; Okada, Etsuji; Albrieux, Florian; Beavogui, Abdoul Habib; Bienvenu, Anne-Lise; Picot, Stephane; Bouillon, Jean-Philippe; Medebielle, Maurice
Journal of Medicinal Chemistry, 2013 , vol. 56, # 1 p. 73 - 83
反应条件
chlorine
T=22.85°C; P=700 Torr; Kinetics; Further Variations:Reagents;
参考文献
Hurley; Wallington; Sulbaek Andersen; Ellis; Martin; Mabury
Journal of Physical Chemistry A, 2004 , vol. 108, # 11 p. 1973 - 1979
反应条件
hydroxide
T=-40.15 - 98.85°C; Oxidation; P=10 - 300 Torr; Kinetics; Further Variations:Reagents;
参考文献
Vesine; Bossoutrot; Mellouki; Le Bras; Wenger; Sidebottom
Journal of Physical Chemistry A, 2000 , vol. 104, # 37 p. 8512 - 8520
反应条件
2,2'-azo-bisisobutyronitrile; copper; zinc
0.133333 h; Ambient temperature;
参考文献
Benefice-Malouet, S.; Blancou, H.; Commeyras, A.
Journal of Fluorine Chemistry, 1993 , vol. 63, # 3 p. 217 - 226
反应条件
hydrogen fluoride; fluorine
参考文献
Du Pont de Nemours and Co.
Patent: US3038941 , 1962 ;
反应条件
lithium aluminium tetrahydride; diethyl ether
Erwaermen des erhaltenen Nonafluorvaleraldehyd-hydrats mit Schwefelsaeure;
参考文献
Minnesote Mining and Mfg. Co.
Patent: US2568500 , 1949 ;