3,3,4,4,5,5,5-六氟戊醇合成路线 （共 13 条）
反应条件
anhydrous butyl ether T=-50°C;
参考文献
Journal of the American Chemical Society, , vol. 79, p. 335
Journal of the Chemical Society, , p. 1764,1765
反应条件
in diethyl ether reaction at -50 - 20°C;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
diethyl ether; magnesium; isopropyl bromide
参考文献
Journal of the American Chemical Society, , vol. 75, p. 6324
反应条件
in further solvent(s) reaction in n-butyl ether at -50°C, 41 hours, 20°C, 24 hours and 60°C, 1 hour;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
in further solvent(s) addition of the grignard solution to the ester (solution in n-butyl ether) at -50°C, stirring at -40°C, 24 hours, warming to 20°C within 24 hours and stirring for 24 hours;;
参考文献
Journal of the Chemical Society, , p. 1748 - 1757
参考文献
Industrial and Engineering Chemistry, , vol. 49, p. 1241,1244
参考文献
Journal of the Chemical Society, , p. 1764,1765
Journal of the American Chemical Society, , vol. 74, p. 1387,1390
参考文献
Journal of the Chemical Society, , p. 1764,1765
反应条件
tetrachloromethane; chlorine T=60°C; unter Bestrahlung mit UV-Licht;
参考文献
McBee et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 1609
反应条件
UV-Licht.Irradiation;
参考文献
McBee et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 1609
