(S) -1-氯-2-丙醇合成路线 (共 15 条)
反应条件
hydrogenchloride; water; lithium chloride in tetrahydrofuran T=-30 - 20°C; 20 h;
参考文献
US2011/130377 A1, ;
Page/Page column 19 ;
反应条件
oxygen; lithium chloride; copper dichloride; [Pd2(MeCOCHCOCHCOMe){(S)-Ph-BINAP}X2] in tetrahydrofuran; water T=25°C; Oxidation; P=760 Torr; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 63, # 9 p. 2790 - 2791
反应条件
phosphate buffer; glyceryl tributyrate 52 h; Ambient temperature;
参考文献
Cambou, Bernard; Klibanov, Alexander M.
Journal of the American Chemical Society, 1984 , vol. 106, # 9 p. 2687 - 2692
反应条件
hydrogenchloride in tetrahydrofuran T=40°C; 6 h;
参考文献
Hamdani; De Jeso; Deleuze; Maillard
Tetrahedron Asymmetry, 1991 , vol. 2, # 9 p. 867 - 870
反应条件
hydrogenchloride; lithium chloride in tetrahydrofuran 2.) -30 deg C, 24 h, r.t.;
参考文献
Najera, Carmen; Yus, Miguel; Seebach, Dieter
Helvetica Chimica Acta, 1984 , vol. <1> 67, # 34 p. 289 - 300
反应条件
hydrogenchloride; (R,R)-[Co(salen)]*GaCl3 in diethyl ether T=0 - 4°C; 1 h;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 9 p. 1862 - 1872
反应条件
Amberlyst in methanol T=40°C; 2 h;
参考文献
Tetrahedron Asymmetry, , vol. 2, # 9 p. 867 - 870
反应条件
1: 1-chloro-propan-2-ol With Candida antarctica lipase B in isopropyl alcohol T=30°C; 0.5 h; Enzymatic reaction; 2: vinyl acetate in isopropyl alcohol T=30°C; 0.0833333 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron, , vol. 65, # 46 p. 9583 - 9591
反应条件
1: 1-chloro-propan-2-ol With Burkholderia cepacia lipase in isopropyl alcohol T=30°C; 0.5 h; Enzymatic reaction; 2: vinyl acetate in isopropyl alcohol T=30°C; 0.266667 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron, , vol. 65, # 46 p. 9583 - 9591
反应条件
baker's yeast in water T=35°C; 72 h; reduction of other 1-chloro-2-alkanones; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 3 p. 631 - 638