2-羟甲基-3,4-二氢吡喃合成路线 (共 17 条)
反应条件
lithium aluminium tetrahydride in diethyl ether T=15°C; 1 h;
参考文献
Fehr, Charles; Galindo, Jose; Ohloff, Guenther
Helvetica Chimica Acta, 1981 , vol. 64, # 5 p. 1247 - 1256
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Nugiel; Cornelius; Corbett
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 201 - 203
反应条件
sodium tetrahydroborate
参考文献
Passacantilli, Pietro
Tetrahedron Letters, 1989 , vol. 30, # 39 p. 5349 - 5352
反应条件
lithium aluminium tetrahydride
参考文献
Tetrahedron, , vol. 46, # 5 p. 1503 - 1514
反应条件
magnesium; methyl iodide 1) diethyl ether, 2) 15 min, r.t; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 204, # 1 p. 11 - 25
反应条件
magnesium 1) diethyl ether, 2) 15 min, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 204, # 1 p. 11 - 25
反应条件
ethyltitanium triisopropoxide in diethyl ether -50 deg C to room temp. over 12 h; Yields of byproduct given;
参考文献
Singh, Shankar M.; Oehlschlager, Allan C.
Canadian Journal of Chemistry, 1988 , vol. 66, p. 209 - 213
反应条件
lithium aluminium tetrahydride in ethylene glycol dimethyl ether 150 h; Heating;
参考文献
Majumdar, K. C.; Ranganayakulu, K.; Brown, R. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 4 p. 303 - 306
反应条件
lithium aluminium tetrahydride in various solvent(s) 16 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 4 p. 303 - 306
反应条件
1: 50 percent / N-bromosuccinimide / CCl4 / 18 h 2: 56 percent / KOH / ethanol / 24 h / Heating View Scheme
参考文献
Blake, Alexander J.; Dawson, Ian M.; Forsyth, Angus C.; Gould, Robert O.; Paton, R. Michael; Taylor, Desmond
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 1 p. 75 - 80