1-(4-甲氧基苯基)-3-苯基脲合成路线 (共 38 条)
反应条件
1: THF-d8 (tetrahydrofuran-d8) / 20 °C
2: chloroform / 0.5 h / 50 °C
View Scheme
参考文献
Rawling, Tristan; McDonagh, Andrew M.; Tattam, Bruce; Murray, Michael
Tetrahedron, 2012 , vol. 68, # 30 p. 6065 - 6070
反应条件
triphenylphosphine
1.) benzene, reflux; Multistep reaction;
参考文献
Corrie, John E.T.; Kirby, Gordon W.; Sharma, Ram P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1571 - 1574
反应条件
1: 1,3,2,4-dioxathiazole S-oxide 12 h; Reflux;
2: aniline T=20°C; 24 h;
参考文献
Mitchell, William R.; Paton, R. Michael
Arkivoc, 2010 , vol. 2010, # 10 p. 34 - 54
反应条件
in acetonitrile
T=25°C; 24 h; Kinetics; Temperature;
参考文献
Sung, Dae Dong; Jang, Hee Man; Jung, Dae Il; Leeb, Ikchoon
Journal of Physical Organic Chemistry, 2008 , vol. 21, # 11 p. 1014 - 1019
反应条件
in acetonitrile
T=25°C; 24 h; Kinetics; Temperature;
参考文献
Sung, Dae Dong; Jang, Hee Man; Jung, Dae Il; Leeb, Ikchoon
Journal of Physical Organic Chemistry, 2008 , vol. 21, # 11 p. 1014 - 1019
反应条件
in acetonitrile
T=25°C; 24 h; Kinetics;
参考文献
Sung, Dae Dong; Jang, Hee Man; Jung, Dae Il; Leeb, Ikchoon
Journal of Physical Organic Chemistry, 2008 , vol. 21, # 11 p. 1014 - 1019
反应条件
in acetonitrile
T=25°C; 24 h; Kinetics;
参考文献
Sung, Dae Dong; Jang, Hee Man; Jung, Dae Il; Leeb, Ikchoon
Journal of Physical Organic Chemistry, 2008 , vol. 21, # 11 p. 1014 - 1019
反应条件
nitrosyl chloride in N,N-dimethyl-formamide
T=0°C; 2 h; further nitrosating agent (N2O3); Product distribution;
参考文献
Miyahara
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 5 p. 1950 - 1960