1-(4-甲氧基苯基)-3-苯基脲合成路线 (共 38 条)
反应条件
1: Et3N / ethyl acetate
2: Et3N / toluene
View Scheme
参考文献
Mukaiyama,T.; Nohira,H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 782 - 784
反应条件
in acetone
6 h; Heating;
参考文献
Beckert, R.; Mayer, R.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 2 p. 227 - 236
参考文献
Naegeli; Tyabji; Conrad
Helvetica Chimica Acta, 1938 , vol. 21, p. 1127,1139
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); t-Bu Brett Phos; triethylamine / toluene / 16 h / 110 °C / Inert atmosphere
2: toluene / 5 h / 60 °C / Inert atmosphere
View Scheme
参考文献
Vinogradova, Ekaterina V.; Fors, Brett P.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2012 , vol. 134, # 27 p. 11132 - 11135
参考文献
Dondoni,A. et al.
Journal of Organic Chemistry, 1977 , vol. 42, # 21 p. 3372 - 3377
反应条件
1: (thermolysis)
2: aq. HCl
View Scheme
参考文献
Dondoni,A. et al.
Journal of Organic Chemistry, 1977 , vol. 42, # 21 p. 3372 - 3377
反应条件
1: 41 percent / tetrahydrofuran / 72 h / 100 °C / 6000480 Torr
View Scheme
参考文献
Azad, Saleha; Kumamoto, Koji; Uegaki, Kaoru; Ichikawa, Yoshiyasu; Kotsuki, Hiyoshizo
Tetrahedron Letters, 2006 , vol. 47, # 4 p. 587 - 590
反应条件
1: benzene
2: toluene; benzene
View Scheme
参考文献
Naegeli; Tyabji; Conrad
Helvetica Chimica Acta, 1938 , vol. 21, p. 1127,1139
参考文献
Miyahara
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 5 p. 1950 - 1960
反应条件
1: 1,2-dichloro-ethane / 18 h / 50 °C / Inert atmosphere
2: chloroform / 0.5 h / 50 °C
View Scheme
参考文献
Rawling, Tristan; McDonagh, Andrew M.; Tattam, Bruce; Murray, Michael
Tetrahedron, 2012 , vol. 68, # 30 p. 6065 - 6070