5-氨基-2,4,6-三碘异酞酰氯合成路线 (共 14 条)
参考文献
Bracco Industria Chimica S.p.A.
Patent: US4352788 A1, 1982 ;
反应条件
in N,N-dimethyl acetamide 16 h; Ambient temperature;
参考文献
Pillai, K. M. R.; Diamantidis, G.; Duncan, L.; Ranganathan, R. S.
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1344 - 1350
反应条件
1: N,N-dimethyl-acetamide / 16 h / Ambient temperature 2: pyridine / 6 h / Ambient temperature View Scheme
参考文献
Pillai, K. M. R.; Diamantidis, G.; Duncan, L.; Ranganathan, R. S.
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1344 - 1350
反应条件
triethylamine in tetrahydrofuran
T=0 - 20°C; 48 h;
参考文献
IMPERIAL INNOVATIONS LIMITED; KINGS COLLEGE LONDON; GUYS AND ST THOMAS NHS FOUNDATION TRUST
Patent: WO2007/26140 A2, 2007 ;
Location in patent: Page/Page column 21; 22 ;