aluminium trichloride in neat (no solvent) addn. of thionyl chloride to Ge compound (pentane, -75°C, N2 or Ar); concn. of solvent, distillation (vac.), elem. anal.;
参考文献
Dousse, G.; Lavayssiere, H.; Satge, J.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1989 , vol. 19, p. 49 - 74
4,4'-diaminostilbene-2,2'-disulfonic acid in diethylene glycol dimethyl ether 0.5 h; Yields of byproduct given;
参考文献
Shellhamer, Dale F.; Anstine, D. Timothy; Gallego, Kelly M.; Ganesh, Brian R.; Hanson, Aaron A.; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 4 p. 861 - 866
4,4'-diaminostilbene-2,2'-disulfonic acid in ethylene glycol dimethyl ether 0.5 h; other diols, var. solv.; Mechanism;
参考文献
Shellhamer, Dale F.; Anstine, D. Timothy; Gallego, Kelly M.; Ganesh, Brian R.; Hanson, Aaron A.; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 4 p. 861 - 866
