3,4-二氢-6-甲基-2H-吡喃-2-酮合成路线 （共 30 条）
反应条件
[(PPh3)AuCl]; silver trifluoromethanesulfonate in dichloromethane T=20°C; 16 h; Inert atmosphere;
参考文献
Muratore, Michael E.; Holloway, Chloe A.; Pilling, Adam W.; Storer, R. Ian; Trevitt, Graham; Dixon, Darren J.
Journal of the American Chemical Society, 2009 , vol. 131, # 31 p. 10796 - 10797
反应条件
acetic anhydride; toluene-4-sulfonic acid in benzene T=0°C; 4 h;
参考文献
Mandal, A.K.; Jawalkar, D.G.
Journal of Organic Chemistry, 1989 , vol. 54, # 10 p. 2364 - 2369
反应条件
lt;(cycphos)RhClgt;2 in dichloromethane 80 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Wakabayashi, Takanori; Ishii, Youichi; Ishikawa, Kazunari; Hidai, Masanobu
Angewandte Chemie, 1996 , vol. 108, # 18 p. 2268 - 2269
反应条件
triethylamine; bis(benzonitrile)palladium(II) dichloride in acetonitrile 5 h; Heating;
参考文献
Wang, Yong-Gang; Wachi, Masaaki; Kobayashi, Yuichi
Synlett, 2006 , # 3 p. 481 - 483
反应条件
sodium acetate; dichloro bis(acetonitrile) palladium(II) in acetonitrile 5 h; Ambient temperature;
参考文献
Annby, Ulf; Stenkula, Magnus; Andersson, Carl-Magnus
Tetrahedron Letters, 1993 , vol. 34, # 52 p. 8545 - 8548
反应条件
1: formyl cyclopropane With C{N(2,6-iPr2C6H3)CH}2 in toluene T=20°C; 4 h; 2: carbon monoxide T=20°C; P=3800.26 Torr; 0.0833333 h;
参考文献
Tamaki, Takashi; Nagata, Midue; Ohashi, Masato; Ogoshi, Sensuke
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10083 - 10091
反应条件
1.1: Br2 / CH2Cl2 / 1.5 h / -60 - -50 °C 1.2: 80 percent / aq. KOH / 10 h / Heating 2.1: Et3N / PdCl2(PhCN)2 / acetonitrile / 5 h / Heating View Scheme
参考文献
Wang, Yong-Gang; Wachi, Masaaki; Kobayashi, Yuichi
Synlett, 2006 , # 3 p. 481 - 483
反应条件
bis(benzonitrile)palladium(II) dichloride; triethylamine in tetrahydrofuran T=60°C; 3 h; Inert atmosphere;
参考文献
Maeno, Zen; Mitsudome, Takato; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Heterocycles, 2012 , vol. 86, # 2 p. 947 - 954
反应条件
mercury(II) trifluoroacetate in dichloromethane 68 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Chan, Dominic M. T.; Marder, Todd B.; Milstein, David; Taylor, Nicholas J.
Journal of the American Chemical Society, 1987 , vol. 109, # 21 p. 6385 - 6388
反应条件
air T=400 - 450°C; Oxidation; Formation of xenobiotics;
参考文献
Park, Byung-Ik; Bozzelli, Joseph W.; Booty, Michael R.; Bernhard, Mary J.; Mesuere, Karel; Pettigrew, Charles A.; Shi, Ji-Chun; Simonich, Staci L.
Environmental Science and Technology, 1999 , vol. 33, # 15 p. 2584 - 2592
