6,6''-二甲基-[2,2':6',2''-三联吡啶]-4'-羧酸乙酯合成路线 （共 4 条）
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in benzene 3 h; Heatingirradiation;
参考文献
Ulrich, Gilles; Bedel, Sebastien; Picard, Claude; Tisnes, Pierre
Tetrahedron Letters, 2001 , vol. 42, # 35 p. 6113 - 6115
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Stille reaction; 48 h; Heating;
参考文献
Bedel, Sebastien; Ulrich, Gilles; Picard, Claude; Tisnes, Pierre
Synthesis, 2002 , # 11 p. 1564 - 1570
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
72 h; Heating;
参考文献
Galaup, Chantal; Couchet, Jean-Marc; Bedel, Sebastien; Tisnes, Pierre; Picard, Claude
Journal of Organic Chemistry, 2005 , vol. 70, # 6 p. 2274 - 2284
反应条件
1: POBr3 / 3 h / 180 °C
2: H2SO4
3: 44 percent / Pd(PPh3)4 / toluene / 48 h / Heating
View Scheme
参考文献
Ulrich, Gilles; Bedel, Sebastien; Picard, Claude; Tisnes, Pierre
Tetrahedron Letters, 2001 , vol. 42, # 35 p. 6113 - 6115
