(氯亚甲基)二甲基氯化铵合成路线 (共 84 条)
反应条件
pyridine
5 h; Heating;
参考文献
Glushenko; Goncharov; Aksenov
Chemistry of Heterocyclic Compounds, 2008 , vol. 44, # 8 p. 973 - 978
反应条件
1: 5-chloro-1,3-dihydro-2H-indol-2-one With phosphorus(III) oxychloride in 1,2-dichloro-ethane
Vilsmeier-Haack-Arnold reaction; 0.5 h; Heating;
2: N-(chloromethylene)-N-methylmethanaminium chloride in 1,2-dichloro-ethane
20 h; Heating;
参考文献
Engqvist, Robert; Javaid, Atif; Bergman, Jan
European Journal of Organic Chemistry, 2004 , # 12 p. 2589 - 2592
反应条件
tetra-n-butylammonium Benzoate
1.) THF 0 deg C, 2.) reflux, 16 h; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G. M.; Braddock, D. Christopher; James, Rachel A.; Koike, Nobuyuki; Procopiou, Panayiotis A.
Journal of Organic Chemistry, 1998 , vol. 63, # 18 p. 6273 - 6280
反应条件
in N,N-dimethyl-formamide
T=150°C; 0.833333 h; Inert atmosphereMicrowave irradiation;
参考文献
Tseng, Ming-Chung; Cheng, Hui-Ting; Shen, Meng-Jane; Chu, Yen-Ho
Organic Letters, 2011 , vol. 13, # 16 p. 4434 - 4437