3-甲氧基氧杂蒽-9-酮合成路线 （共 39 条）
反应条件
sulfuric acid
T=100°C;
参考文献
Ullmann; Wagner
Justus Liebigs Annalen der Chemie, 1907 , vol. 355, p. 366
Justus Liebigs Annalen der Chemie, 1909 , vol. 371, p. 388
反应条件
sulfuric acid
T=50°C; 1 h;
参考文献
Passarotti; Valenti; Grianti; Marini
Bollettino Chimico Farmaceutico, 1994 , vol. 133, # 9 p. 592 - 596
反应条件
methanol; potassium hydroxide
T=100°C; im Druckrohr;
参考文献
Dreher; v. Kostanecki
Chemische Berichte, 1893 , vol. 26, p. 75
反应条件
tin(IV) chloride
T=130°C;
参考文献
Neunhoeffer; Haase
Chemische Berichte, 1958 , vol. 91, p. 1801,1804
反应条件
1: potassium carbonate / N,N-dimethyl acetamide / 6 h / 170 °C / |Inert atmosphere
2: tetrabutylammomium bromide; tert.-butylhydroperoxide / water / 24 h / 120 °C / |Schlenk technique; |Sealed tube
View Scheme
参考文献
Rao, Honghua; Ma, Xinyi; Liu, Qianzi; Li, Zhongfeng; Cao, Shengli; Li, Chao-Jun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 11-12 p. 2191 - 2196
反应条件
pyridine; aluminium trichloride; tetreamethyl ammonium hydroxide
1.) Et2O, RT, 8 h, 2.) H2O, reflux, 36 h; Yield given. Multistep reaction;
参考文献
Lin; Liou; Ko; Teng
Journal of Pharmaceutical Sciences, 1993 , vol. 82, # 1 p. 11 - 16
反应条件
sulfuric acid
Diazotization;
参考文献
Ullmann; Denzler
Chemische Berichte, 1906 , vol. 39, p. 4337
反应条件
ethanol; nickel
Hydrogenation;
参考文献
Mittal; Seshadri
Journal of Scientific and Industrial Research, 1955 , vol. 14 B, p. 76
反应条件
1: phosphorus pentachloride; carbon disulfide / das Chlorid mit Resorcindimethylaether und Aluminiumchlorid erwaermen
2: glacial acetic acid; concentrated sulfuric acid
3: sulfuric acid / Diazotization
View Scheme
参考文献
Ullmann; Denzler
Chemische Berichte, 1906 , vol. 39, p. 4337
反应条件
1: potassium carbonate; acetone
2: Raney nickel; ethanol / Hydrogenation
View Scheme
参考文献
Mittal; Seshadri
Journal of Scientific and Industrial Research, 1955 , vol. 14 B, p. 76
