3-甲氧基氧杂蒽-9-酮合成路线 （共 39 条）
反应条件
pyridine hydrochloride T=180 - 200°C; 2 h;
参考文献
Sato; Dan; Onuma; Tanaka; Koga
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 5 p. 1266 - 1277
参考文献
Ullmann; Wagner
Justus Liebigs Annalen der Chemie, 1907 , vol. 355, p. 366
Justus Liebigs Annalen der Chemie, 1909 , vol. 371, p. 388
Full Text Show Details
Ullmann; Denzler
Chemische Berichte, 1906 , vol. 39, p. 4337
反应条件
hydrogenchloride; acetic acid T=60°C; 2 h;
参考文献
Passarotti; Valenti; Grianti; Marini
Bollettino Chimico Farmaceutico, 1994 , vol. 133, # 9 p. 592 - 596
反应条件
1: 9 g / AcOH, aq. HCl / 2 h / 60 °C 2: 89 percent / dimethylformamide / 2 h / Ambient temperature View Scheme
参考文献
Passarotti; Valenti; Grianti; Marini
Bollettino Chimico Farmaceutico, 1994 , vol. 133, # 9 p. 592 - 596
反应条件
sodium hydroxide in methanol; water
Heating;
参考文献
Fernandes, Carla; Masawang, Kamonporn; Tiritan, Maria Elizabeth; Sousa, Emilia; De Lima, Virginia; Afonso, Carlos; Bousbaa, Hassan; Sudprasert, Wanwisa; Pedro, Madalena; Pinto, Madalena M.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 3 p. 1049 - 1062
反应条件
pyridine; tetreamethyl ammonium hydroxide in water
36 h; Reflux;
参考文献
Cheng, Jen-Hao; Huang, A-Mei; Hour, Tzyh-Chyuan; Yang, Shyh-Chyun; Pu, Yeong-Shiau; Lin, Chun-Nan
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 4 p. 1222 - 1231
反应条件
aluminium trichloride; sodium methylate
1) 1,2-dichloroethane, a) 0-5 deg C up to r.t. over 3 h, b) refl., 1 h, 2) MeOH, EtOH, refl., 1 h; Yield given. Multistep reaction;
参考文献
Sato; Dan; Onuma; Tanaka; Koga
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 5 p. 1266 - 1277
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in N,N-dimethyl-formamide
T=130°C; 12 h; Inert atmosphere;
参考文献
Wang, Sizhuo; Xie, Kai; Tan, Ze; An, Xiangyu; Zhou, Xingjian; Guo, Can-Cheng; Peng, Zhihong
Chemical Communications, 2009 , # 42 p. 6469 - 6471
反应条件
cesium fluoride in tetrahydrofuran
T=90°C; 24 h;
参考文献
Zhao, Jian; Larock, Richard C.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 583 - 588
反应条件
sulfuric acid; acetic anhydride
参考文献
Goldberg; Wragg
Journal of the Chemical Society, 1958 , p. 4227,4230
