3-羟基-7,8,9,10-四氢苯并[c]苯并吡喃-6-酮合成路线 （共 18 条）
反应条件
1: K2CO3 / acetone / 50 - 56 °C 2: aq. NaOH / Heating View Scheme
参考文献
Dubovik; Garazd; Vinogradova; Khilya
Chemistry of Natural Compounds, 2006 , vol. 42, # 2 p. 133 - 137
反应条件
in 1,4-dioxane T=100°C; Mannich reaction;
参考文献
Garazd; Panteleimonova; Khilya
Chemistry of Natural Compounds, 2002 , vol. 38, # 6 p. 532 - 538
反应条件
in 1,4-dioxane T=100°C; Mannich reaction;
参考文献
Garazd; Panteleimonova; Khilya
Chemistry of Natural Compounds, 2002 , vol. 38, # 6 p. 532 - 538
反应条件
sulfuric acid
T=0 - 20°C; Pechmann condensation; 1 h;
参考文献
Fusegi, Keiko; Kumamoto, Takuya; Nakanishi, Waka; Ishikawa, Tsutomu
Heterocycles, 2009 , vol. 77, # 1 p. 603 - 610
反应条件
sulfuric acid in ethyl acetate
T=20°C; 12 h;
参考文献
Wyatt, Emma E.; Fergus, Suzanne; Galloway, Warren R. J. D.; Bender, Andreas; Fox, David J.; Plowright, Alleyn T.; Jessiman, Alan S.; Welch, Martin; Spring, David R.
Chemical Communications, 2006 , # 31 p. 3296 - 3298
反应条件
Bi(NO3)3·5H2O
T=80°C; Pechmann Condensation;
参考文献
Chen, Yin; Lan, Yu; Wang, Songlin; Zhang, Heng; Xu, Xiangqing; Liu, Xin; Yu, Minquan; Liu, Bi-Feng; Zhang, Guisen
European Journal of Medicinal Chemistry, 2014 , vol. 74, p. 427 - 439
反应条件
methanesulfonic acid
15 deg C to RT, 15 min;
参考文献
Collins, David J.; Fallon, Gary D.; Staffa, Alfred; Tope, Helen
Australian Journal of Chemistry, 1996 , vol. 49, # 6 p. 719 - 721
反应条件
1: sulfuric acid / |Reflux
2: AlCl3, aluminium chloride; triethylamine / dichloromethane / 0 - 20 °C
3: Bi(NO3)3·5H2O / 80 °C
View Scheme
参考文献
Chen, Yin; Lan, Yu; Wang, Songlin; Zhang, Heng; Xu, Xiangqing; Liu, Xin; Yu, Minquan; Liu, Bi-Feng; Zhang, Guisen
European Journal of Medicinal Chemistry, 2014 , vol. 74, p. 427 - 439
反应条件
1: AlCl3, aluminium chloride; triethylamine / dichloromethane / 0 - 20 °C
2: Bi(NO3)3·5H2O / 80 °C
View Scheme
参考文献
Chen, Yin; Lan, Yu; Wang, Songlin; Zhang, Heng; Xu, Xiangqing; Liu, Xin; Yu, Minquan; Liu, Bi-Feng; Zhang, Guisen
European Journal of Medicinal Chemistry, 2014 , vol. 74, p. 427 - 439
反应条件
1: aqueous sulfuric acid
2: Erhitzen auf Temperaturen oberhalb des Schmelzpunkts
View Scheme
参考文献
Desai et al.
Proceedings - Indian Academy of Sciences, Section A, 1947 , # 25 p. 345,347
