sulfur in neat (no solvent)
reaction with an excess of sulfur in an autoclave at 200-280°C;;
参考文献
Emeleus, H. J.
Fortschr. Chem. Forsch., 1951 , vol. 2, p. 609 - 618
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Emeleus, H. J.
Suomen Kemistilehti B, 1958 , vol. 31, p. 101 - 109
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Gmelin Handbook: C: MVol.D2, 4.2.4.4.5, page 319 - 320
SCl2 in xylene
0.75 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Munavalli, Shekar; Rossman, David I.; Rohrbaugh, Dennis K.; Ferguson, C. Parker; Szafraniec, Leonard J.
Journal of Fluorine Chemistry, 1992 , vol. 59, # 1 p. 91 - 99
byproducts: CF3SH, S, KF*HF; warming to 25°C in the presence of excess KF;
参考文献
Burton,C.A.; Shreeve,J.M.
Journal of the American Chemical Society, 1976 , vol. 98, p. 6545 - 6547
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Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
byproducts: CF3SH, S, CsF*HF; warming to 25°C in the presence of excess CsF;
参考文献
Burton,C.A.; Shreeve,J.M.
Journal of the American Chemical Society, 1976 , vol. 98, p. 6545 - 6547
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
