反应条件
in 1,4-dioxane
byproducts: Me3SiCl, Me3SiOSiMe2OSiMe3, Me3SiOSiMe2Cl; mixt. of dichlorogermylene and siloxane in dioxane stirred for 29 h at 85-95°C with barbotage of air; liq. phase distilled at atm. pressure and in vaq.;
参考文献
Shcherbinin; Pushkina; Krivolapova; Bykovchenko; Khromykh; Komalenkova; Chernyshev
Russian Journal of General Chemistry, 2002 , vol. 72, # 12 p. 1907 - 1910