反应条件
(C2H5)3N in toluene byproducts: (C2H5)3NHCl; slow dropwise addn. of (C6H5)4Ge2Cl2 (in toluene) to soln. of (HO)2Ge(C(CH3)3)2 and N(C2H5)3 in toluene; stirring (room temp./1-2 h);; filtration from (C2H5)3NHCl; concn.; recrystn. (petroleum ether); removal of (C6H5)8Ge4O2 by fractionated crystn.; elem. anal.;;
参考文献
Puff, Heinrich; Heising, Heribert; Schuh, Willi; Schwab, Werner
Journal of Organometallic Chemistry, 1986 , vol. 303, p. 343 - 350
