2-(甲基硫代)苯甲酸甲酯合成路线 (共 49 条)
反应条件
dihydrogen peroxide; Mg-Al-LDH-WO4 T=20°C; 3 h;
参考文献
Choudary; Bharathi; Venkat Reddy; Lakshmi Kantam
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 18 p. 2069 - 2074
参考文献
Fletcher; Namkung; Pan; Cole
Journal of medicinal chemistry, 1971 , vol. 14, # 11 p. 1113 - 1115
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-78 - 20°C;
参考文献
FAB PHARMA SAS; GERUSZ, Vincent; ESCAICH, Sonia; OXOBY, Mayalen; DENIS, Alexis
Patent: WO2011/61214 A1, 2011 ;
Location in patent: Page/Page column 159 ;
WO 2011/061214 A1
参考文献
Chatterjea; Prasad
Journal of the Indian Chemical Society, 1954 , vol. 31, p. 203,208
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=75°C;
参考文献
Huynh, Han Vinh; Yeo, Chun Hui; Chew, Ying Xia
Organometallics, 2010 , vol. 29, # 6 p. 1479 - 1486
反应条件
lithium diisopropyl amide in tetrahydrofuran T=0 - 20°C; 2 h;
参考文献
Cabiddu, M. Grazia; Cabiddu, Salvatore; Cadoni, Enzo; De Montis, Stefania; Fattuoni, Claudia; Melis, Stefana; Usai, Michele
Synthesis, 2002 , # 7 p. 875 - 878
反应条件
magnesium in diethyl ether
1 h; Heating;
参考文献
Ruff, Ferenc; Kucsman, Arpad
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1123 - 1128
反应条件
1: in diethyl ether
T=25°C; Grignard reaction; 3 h; Reflux;
2: With sulfuric acid; water in diethyl ether
Cooling with ice;
参考文献
Prusek, Ondrej; Bures, Filip; Pytela, Oldrich
Collection of Czechoslovak Chemical Communications, 2009 , vol. 74, # 1 p. 85 - 99
反应条件
tetrachloromethane; N-bromosuccinmide
参考文献
Groebel
Chemische Berichte, 1959 , vol. 92, p. 2887,2891