(-)-二甲基-2,3-邻异丙亚基-L-酒石酸酯合成路线 （共 28 条）
参考文献
Gherase, Dragos; Roussel, Christian
Central European Journal of Chemistry, 2012 , vol. 10, # 4 p. 1066 - 1072
反应条件
2: pyridine 3: NaI / butan-2-one / Heating 4: H2/NEt3 / 5percent Pd/C / methanol View Scheme
参考文献
Ortunno, R. M.; Alonso, D.; Font, J.
Tetrahedron Letters, 1986 , vol. 27, # 9 p. 1079 - 1080
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 1.25 h;
参考文献
Zang, Qin; Gulab, Shivali; Stocker, Bridget L.; Baars, Sylvia; Hoberg, John O.
European Journal of Organic Chemistry, 2011 , # 23 p. 4465 - 4471
反应条件
1: 94 percent / NH3 / methanol 2: 77 percent / LiAlH4 / tetrahydrofuran / Heating View Scheme
参考文献
Star, Alexander; Goldberg, Israel; Lemcoff, N. Gabriel; Fuchs, Benzion
European Journal of Organic Chemistry, 1999 , # 9 p. 2033 - 2043
反应条件
1: 85 percent / AlMe3 / CH2Cl2 / -10 °C 2: 47 percent / tetrahydrofuran View Scheme
参考文献
European Journal of Organic Chemistry, , # 6 p. 1455 - 1467
反应条件
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 °C / Reflux; Inert atmosphere 2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.75 h / 0 - 20 °C 2.2: 16 h / 20 °C 3.1: 1H-imidazole; iodine; triphenylphosphine / toluene; acetonitrile / 1 h / 60 °C 4.1: Pearlman's catalist; hydrogen; triethylamine / methanol / 24 h / 20 °C / 760.05 Torr View Scheme
参考文献
Davies, Stephen G.; Foster, Emma M.; Frost, Aileen B.; Lee, James A.; Roberts, Paul M.; Thomson, James E.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 30 p. 6186 - 6200
反应条件
1: 88 percent / LiAlH4 / tetrahydrofuran
2: 95 percent / pyridine
3: 94.5 percent / NaI / acetone / Heating
View Scheme
参考文献
Khanapure, Subhash P.; Najafi, Nahid; Manna, Sukumar; Yang, Jing-Jing; Rokach, Joshua
Journal of Organic Chemistry, 1995 , vol. 60, # 23 p. 7548 - 7551
反应条件
in methanol
96 h; Ambient temperature;
参考文献
Ito, Yoshio N.; Ariza, Xavier; Beck, Albert K.; Bohac, Andrej; Ganter, Camille; et al.
Helvetica Chimica Acta, 1994 , vol. 77, # 8 p. 2071 - 2110
