2,4-二氯-6-异丙基氨基-1,3,5-三嗪合成路线 （共 6 条）
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran
参考文献
Synaptic Pharmaceutical Corporation
Patent: US6340683 B1, 2002 ;
Location in patent: Page column 17 ;
US 6340683 B1
反应条件
1: sodium hydroxide / water; toluene / 0.25 h / 15 - 20 °C 2: tetrahydrofuran; water / 24 h / Reflux View Scheme
参考文献
Zhao, Huaping; Liu, Yuxiu; Cui, Zhipeng; Beattie, David; Gu, Yucheng; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2011 , vol. 59, # 21 p. 11711 - 11717
参考文献
Barton, Benita; Gouws, Shawn; Schaefer, Melissa C.; Zeelie, Bernard
Organic Process Research and Development, 2003 , vol. 7, # 6 p. 1071 - 1076
反应条件
sodium hydroxide in water; toluene T=15 - 20°C; 0.25 h;
参考文献
Zhao, Huaping; Liu, Yuxiu; Cui, Zhipeng; Beattie, David; Gu, Yucheng; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2011 , vol. 59, # 21 p. 11711 - 11717
反应条件
in tetrahydrofuran
T=-10 - 20°C; 0.5 h;
参考文献
Zhao, Huaping; Liu, Yuxiu; Cui, Zhipeng; Beattie, David; Gu, Yucheng; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2011 , vol. 59, # 21 p. 11711 - 11717
反应条件
sodium hydroxide in ethyl acetate
参考文献
Ciba-Geigy Corporation
Patent: US4220770 A1, 1980 ;
