三(2,2,2-三氟乙基)亚磷酸酯合成路线 （共 26 条）
反应条件
pyridine; phosphorus trichoride in diethyl ether 1.) -10 deg C, 1 h, 2.) reflux, 1 h;
参考文献
Leeuwen, P. W. N. M. van; Roobeek, C. F.
Tetrahedron, 1981 , vol. 37, p. 1973 - 1984
参考文献
Mironov, V. F.; Konovalova, I. V.
Russian Journal of General Chemistry, 1993 , vol. 63, # 10.1 p. 1548 - 1550
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 10 p. 2228 - 2232
参考文献
Mironov, V. F.; Konovalova, I. V.
Russian Journal of General Chemistry, 1993 , vol. 63, # 10.1 p. 1548 - 1550
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 10 p. 2228 - 2232
反应条件
phosphorus trichoride 1.) -5 deg C, 4 h, 2.) from -5 deg C to RT, 1 h;
参考文献
Luo; Atrazheva; Fregeau; Gmeiner; Lown
Canadian Journal of Chemistry, 1994 , vol. 72, # 6 p. 1548 - 1555
反应条件
other bis(fluoroalkyl) hydrogen phosphites; Mechanism;
参考文献
Mironov, V. F.; Konovalova, I. V.
Russian Journal of General Chemistry, 1993 , vol. 63, # 10.1 p. 1548 - 1550
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 10 p. 2228 - 2232
反应条件
PAIBN in acetonitrile-D3 T=15°C; 0.166667 h; UV-irradiation; Time;
参考文献
Journal of Organic Chemistry, , vol. 78, # 8 p. 3561 - 3569
反应条件
cyclohexane-1,2-epoxide in neat (no solvent) T=34°C; 4.16667 h; UV-irradiation;
参考文献
Journal of Organic Chemistry, , vol. 78, # 8 p. 3561 - 3569
反应条件
cyclohexane-1,2-epoxide in acetonitrile-D3 T=34°C; 4.5 h; UV-irradiation;
参考文献
Journal of Organic Chemistry, , vol. 78, # 8 p. 3561 - 3569
反应条件
tetrahydrofuran; PAIBN T=30°C; 1 h; UV-irradiation;
参考文献
Journal of Organic Chemistry, , vol. 78, # 8 p. 3561 - 3569
反应条件
in acetonitrile-D3 T=15°C; 0.166667 h; UV-irradiation; TimeConcentration;
参考文献
Journal of Organic Chemistry, , vol. 78, # 8 p. 3561 - 3569
