1,3-二甲氧基-2-丙-2-烯基苯合成路线 （共 19 条）
反应条件
1: ethanolic KOH 2: Na2Cr2O7; aqueous H2SO4; sulfanilic acid View Scheme
参考文献
Schamschurin
Zhurnal Obshchei Khimii, 1944 , vol. 14, p. 211,213
Chem.Abstr., 1945 , p. 2286
反应条件
1: ethanolic KOH 2: Na2Cr2O7; aqueous H2SO4; sulfanilic acid 3: AlCl3; benzene 4: AlCl3; benzene View Scheme
参考文献
Schamschurin
Zhurnal Obshchei Khimii, 1944 , vol. 14, p. 211,213
Chem.Abstr., 1945 , p. 2286
反应条件
1: ethanolic KOH 2: Na2Cr2O7; aqueous H2SO4; sulfanilic acid 3: AlCl3; benzene View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 14, p. 211,213
Chem.Abstr., , p. 2286
反应条件
copper(I) oxide; palladium diacetate; dimethyl sulfoxide; silver carbonate in toluene
T=110°C; 2 h; chemoselective reaction;
参考文献
Wang, Jiantao; Cui, Zili; Zhang, Yuexia; Li, Huajie; Wu, Long-Min; Liu, Zhongquan
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 3 p. 663 - 666
反应条件
2,6-di-tert-butyl-4-methyl-phenol; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride in N,N-dimethyl-formamide
T=120°C; 5.5 h;
参考文献
Saa, Jose M.; Martorell, Gabriel; Garcia-Raso, Angel
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 678 - 685
反应条件
1: 1,3-dimethoxy benzene With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; cobalt(II) dibromide in tetrahydrofuran; hexane
T=0 - 20°C; 0.5 h;
2: allyl bromide in tetrahydrofuran; hexane
T=20°C; 0.5 h;
3: With water in tetrahydrofuran; hexane
参考文献
Dayaker, Gandrath; Chevallier, Floris; Gros, Philippe C.; Mongin, Florence
Tetrahedron, 2010 , vol. 66, # 46 p. 8904 - 8910
反应条件
bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride
参考文献
Martorell, Gabriel; Garcia-Raso, Angel; Saa, Jose M.
Tetrahedron Letters, 1990 , vol. 31, # 16 p. 2357 - 2360
反应条件
1: 1-(allyloxy)-3-methoxybenzene T=180°C; Claisen rearrangement; 10 h;
2: Me-X With potassium carbonate in acetone
参考文献
Akhtar, Yasmin; Yu, Yang; Isman, Murray B.; Plettner, Erika
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 8 p. 4983 - 4991
反应条件
1: potassium carbonate / acetone
2: 10 h / 180 °C
View Scheme
参考文献
Akhtar, Yasmin; Yu, Yang; Isman, Murray B.; Plettner, Erika
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 8 p. 4983 - 4991
反应条件
1: potassium carbonate / acetone
2: potassium carbonate / acetone
3: 10 h / 180 °C
View Scheme
参考文献
Akhtar, Yasmin; Yu, Yang; Isman, Murray B.; Plettner, Erika
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 8 p. 4983 - 4991
