2-[(4-氰基苯基)亚甲基]丙二腈合成路线 (共 5 条)
反应条件
in acetonitrile T=20°C; Reduction; oxidation; 15 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 9 p. 1857 - 1861
反应条件
potassium hydroxide in water; dimethyl sulfoxide T=20°C; different concentrations of solvents; Equilibrium constantRate constant;
参考文献
Bernasconi, Claude F.; Fox, John P.; Kanavarioti, Anastassia; Panda, Markandeswar
Journal of the American Chemical Society, 1986 , vol. 108, # 9 p. 2372 - 2381
反应条件
1: With acetic acid in acetonitrile
0.166667 h;
2: With ammonium acetate in acetonitrile
T=80°C; 8 h;
参考文献
Borate, Hanumant B.; Gaikwad, Supriya H.; Kudale, Ananada S.; Chavan, Subhash P.; Pharande, Shrikant G.; Wagh, Vitthal D.; Sawant, Vikram S.
Tetrahedron Letters, 2013 , vol. 54, # 12 p. 1528 - 1530
反应条件
calcite grains
Knoevenagel condensation; 0.5 h; ball-milling conditions; Product distribution; Further Variations:Reagents;
参考文献
Wada, Shinobu; Suzuki, Hitomi
Tetrahedron Letters, 2003 , vol. 44, # 2 p. 399 - 401
反应条件
air; silica gel
T=90°C; 0.5 h; neat (no solvent);
参考文献
Yu, Chuanming; Guo, Peng; Jin, Can; Su, Weike
Journal of Chemical Research, 2009 , # 5 p. 333 - 336