反应条件
in diethyl ether
a soln. of C4H9MgCl in diethyl ether was slowly added to a soln. of BiCl3 in diethyl ether, after complete addn. the mixt. was slowly cooled to room temp. and allowed to stir for 18 h; filtered, volatiles were removed in vac., pentane was added, filtered, volatiles were removed in vac.;
参考文献
Wooten, Alfred J.; Werder, Donald J.; Williams, Darrick J.; Casson, Joanna L.; Hollingsworth, Jennifer A.
Journal of the American Chemical Society, 2009 , vol. 131, # 44 p. 16177 - 16188
