1-氮杂双环[2.2.2]辛烷-8-醇合成路线 (共 3 条)
反应条件
di-isopropyl azodicarboxylate; 9-azanoradamantane N-oxyl; acetic acid in dichloromethane T=20°C; 8 h;
参考文献
Journal of Organic Chemistry, , vol. 77, # 6 p. 3005 - 3009
参考文献
Brossat, Maude; Moody, Thomas S.; Taylor, Stephen J.C.; Wiffen, Jonathan W.
Tetrahedron Asymmetry, 2009 , vol. 20, # 18 p. 2112 - 2116
反应条件
1: With dimethylsulfide; triethylamine in chloroform T=-15 - -10°C; Inert atmosphere; 2: With N-chloro-succinimide in chloroform T=-15 - -10°C; 4 h; Inert atmosphere;
参考文献
Chavakula, Ramadas; Rao, Mutyala Narayana; Rao, Chennupati Srinivasa
Journal of the Indian Chemical Society, 2013 , vol. 90, # 2 p. 261 - 262