1,2-双(2-碘乙氧基)乙烷合成路线 (共 32 条)
反应条件
sodium carbonate in acetonitrile
27 h; Heating;
参考文献
Gatto, Vincent J.; Arnold, Kristin A.; Viscariello, Anthony M.; Miller, Steven R.; Morgan, Charles R.; Gokel, George W.
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5373 - 5384
反应条件
potassium carbonate in acetonitrile
48 h; Heating;
参考文献
Krakowiak, Krzysztof E.; Maas, Garren E.; Bradshaw, Jerald S.; Hathaway, Jon K.; Izatt, Reed M.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 1 p. 179 - 182
反应条件
sodium carbonate in acetonitrile
36 h; Heating;
参考文献
Krakowiak, Krzysztof E.; Bradshaw, Jerald S.; Izatt, Reed M.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 4 p. 1011 - 1014
反应条件
1: Na2CO3 / acetonitrile
2: methanol
View Scheme
参考文献
Kulstad,S.; Malmsten,L.A.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1979 , vol. 33, p. 469 - 474
反应条件
1: Na2CO3 / acetonitrile
2: Et3N / ethanol
View Scheme
参考文献
Kulstad,S.; Malmsten,L.A.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1979 , vol. 33, p. 469 - 474
参考文献
Gatto, Vincent J.; Arnold, Kristin A.; Viscariello, Anthony M.; Miller, Steven R.; Morgan, Charles R.; Gokel, George W.
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5373 - 5384
反应条件
potassium carbonate in acetone
Heating;
参考文献
Castellan, Alain; Daney, Michele; Desvergne, Jean-Pierre; Riffaud, Marie-Helene; Bouas-Laurent, Henri
Tetrahedron Letters, 1983 , vol. 24, # 47 p. 5215 - 5218
反应条件
sodium carbonate; sodium iodide in ethanol
260 h; Heating;
参考文献
Junek, Hans; Biza, Peter; Geringer, Michael
Monatshefte fuer Chemie, 1992 , vol. 123, # 6 p. 581 - 586
反应条件
1: 30 percent / acetonitrile / 18 h / Heating
2: 87 percent / dicyklohexylcarbodiimid / CH2Cl2 / 20 h / 20 °C
3: 91 percent / palladium / methanol
View Scheme
参考文献
Luk'yanenko, N. G.; Bogat-skii, A. V.; Basok, S. S.; Ostrovskaya, L. K.; Nazarova, N. Yu.; Karpenko, L. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 7 p. 1438 - 1444
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 7 p. 1580 - 1587
反应条件
in N,N-dimethyl-formamide
T=80°C; 5 h;
参考文献
Bottino, Francesco; Grazia, Michele Di; Finocchiaro, Paolo; Fronczek, Frank R.; Mamo, Antonino; Pappalardo, Sebastiano
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3521 - 3529