1,2-双(2-碘乙氧基)乙烷合成路线 (共 32 条)
反应条件
potassium iodide in acetone T=40°C;
参考文献
Aoki, Yuko; Umezawa, Naoki; Asano, Yuko; Hatano, Keiichiro; Yano, Yuki; Kato, Nobuki; Higuchi, Tsunehiko
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 22 p. 7108 - 7115
反应条件
potassium iodide in acetone T=40°C; 96 h;
参考文献
Zhao, Ya-Nan; Yang, Zhen-Zhen; Luo, Si-Hang; He, Liang-Nian
Catalysis Today, 2013 , vol. 200, # 1 p. 2 - 8
反应条件
sodium iodide in acetone Reflux;
参考文献
Jensen, Marie; Schmidt, Steffen; Fedosova, Natalya U.; Mollenhauer, Jan; Jensen, Henrik H.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 7 p. 2407 - 2417
反应条件
sodium iodide in acetone 24 h; Heating;
参考文献
Crossley, Roger; Goolamali, Zia; Gosper, Jeffrey J.; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 3 p. 513 - 520
反应条件
1: pyridine / CH2Cl2 2: 85 percent / NH4I / dimethylformamide / 5 h / 80 °C View Scheme
参考文献
Provencher-Mandeville, Josee; Debnath, Chhanda; Mandal, Sanat K.; Leblanc, Valerie; Parent, Sophie; Asselin, Eric; Berube, Gervais
Steroids, 2011 , vol. 76, # 1-2 p. 94 - 103
反应条件
1: 72 percent / Na2CO3, NaI / acetonitrile / 19 h / Heating 2: 91 percent / H2 / 10 Pd/C / ethanol / 24 h / 25 °C / 3620.04 Torr View Scheme
参考文献
Gatto, Vincent J.; Arnold, Kristin A.; Viscariello, Anthony M.; Miller, Steven R.; Gokel, George W.
Tetrahedron Letters, 1986 , vol. 27, # 3 p. 327 - 330
反应条件
sodium carbonate in acetonitrile 48 h; Heating;
参考文献
Krakowiak, Krzysztof E.; Maas, Garren E.; Bradshaw, Jerald S.; Hathaway, Jon K.; Izatt, Reed M.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 1 p. 179 - 182
反应条件
1: 82 percent / acetone / 20 h / 25 °C / 7500600 Torr 2: 80 percent / triphenylphosphine / dimethylformamide / 5 h / Heating View Scheme
参考文献
Pietraszkiewicz, Marek; Salanski, Piotr; Jurczak, Janusz
Bulletin of the Polish Academy of Sciences, Chemistry, 1985 , vol. 33, # 9-10 p. 433 - 436
反应条件
1: 100 percent / acetone / 20 h / 25 °C / 7500600 Torr 2: 71 percent / triphenylphosphine / dimethylformamide / 5 h / Heating View Scheme
参考文献
Bulletin of the Polish Academy of Sciences, Chemistry, , vol. 33, # 9-10 p. 433 - 436
反应条件
sodium carbonate; sodium iodide in acetonitrile Heating;
参考文献
Gatto, Vincent J.; Arnold, Kristin A.; Viscariello, Anthony M.; Miller, Steven R.; Gokel, George W.
Tetrahedron Letters, 1986 , vol. 27, # 3 p. 327 - 330