n-C4H9 in diethyl ether under N2 Ph3GeH was trated with n-BuLi in ether soln. and was added to a soln. of Co-complex in ether at-78°C, stood for 16 h, evapd., H2O was added, treated with Et3OBF4; extd. with ether, dried over Na2SO4, chromd. (silica gel, toluene), crystd. from C6H6/hexane;
参考文献
Cerveau, Genevieve; Colomer, Ernesto; Corriu, Robert J.P.; Young, J. Colin
Journal of Organometallic Chemistry, 1981 , vol. 205, # 1 p. 31 - 45
