1-(1,2-二苯基乙基)哌啶 (2Z)-2-丁烯二酸盐(1:1)合成路线 (共 11 条)
反应条件
chloro-trimethyl-silane; diisopropylamine; zinc in benzene T=20°C; 6 h;
参考文献
Hatano, Bunpei; Nagahashi, Keita; Kijima, Tatsuro
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 9188 - 9191
反应条件
1: With trifluoroacetic acid; zinc in acetonitrile Mannich type reaction; 1.5 h; Inert atmosphere; 2: With ammonium chloride in water; acetonitrile
参考文献
Le Gall, Erwan; Haurena, Caroline; Sengmany, Stephane; Martens, Thierry; Troupel, Michel
Journal of Organic Chemistry, 2009 , vol. 74, # 20 p. 7971 - 7973
反应条件
1: mercury (II)-chloride; calcium sulfate 2: diethyl ether View Scheme
参考文献
Stewart; Hauser
Journal of the American Chemical Society, 1955 , vol. 77, p. 1098,1100
反应条件
potassium carbonate in acetonitrile T=20°C; 72 h; Inert atmosphere;
参考文献
Berger, Michael L.; Schweifer, Anna; Rebernik, Patrick; Hammerschmidt, Friedrich
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 9 p. 3456 - 3462
反应条件
1: potassium carbonate 2: diethyl ether View Scheme
参考文献
Stewart; Hauser
Journal of the American Chemical Society, 1955 , vol. 77, p. 1098,1100
反应条件
1: mercury (II)-chloride; calcium sulfate 2: diethyl ether View Scheme
参考文献
Stewart; Hauser
Journal of the American Chemical Society, 1955 , vol. 77, p. 1098,1100
参考文献
Stewart; Hauser
Journal of the American Chemical Society, 1955 , vol. 77, p. 1098,1100
反应条件
in acetonitrile T=20°C; 3 h;
参考文献
Le Gall, Erwan; Troupel, Michel; Nedelec, Jean-Yves
Tetrahedron, 2006 , vol. 62, # 42 p. 9953 - 9965
反应条件
1: AuCl(P(C10H15)2C6H4NC4H8O); silver tetrakis(pentafluorophenyl)borate / toluene / 16 h / 110 °C / Inert atmosphere; Sealed cap 2: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 20 °C View Scheme
参考文献
Hesp, Kevin D.; Stradiotto, Mark
Journal of the American Chemical Society, 2010 , vol. 132, # 51 p. 18026 - 18029
参考文献
Christiaen
Bulletin des Societes Chimiques Belges, 1924 , vol. 33, p. 484
Chem. Zentralbl., 1925 , vol. 96, # I p. 388