1,1,2,2-四甲基-二膦合成路线 （共 33 条）
参考文献
Kischkel, Helmut; Roeschenthaler, Gerd-Volker
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 94
反应条件
magnesium
T=296.9 - 346.9°C;
参考文献
Bock, Hans
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 49/50, p. 3 - 53
反应条件
above 600 deg C, pressure lower than 10-3 mmHg; other triazaphosphole; Mechanism;
参考文献
Diallo, O. S.; Lopez, L.; Barrans, J.
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 49/50, p. 363 - 366
反应条件
1: 1,1,2,2-tetramethyldiphosphane With sodium in ammonia
T=-78°C; 1 h;
2: 1-Amino-3-chloro-propane hydrochloride in ammonia
Further stages.;
参考文献
Suzuki, Takayoshi; Fujiiwara, Katsuhiro; Takagi, Hideo D.; Kashiwabara, Kazuo
Dalton Transactions, 2007 , # 3 p. 308 - 319
参考文献
Dehnert,P. et al.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1979 , vol. 34, p. 1646 - 1652
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.2, page 14 - 30
反应条件
in deuterated toluene
starting materials are dissolved in toluene-d8, mixt. is heated at 120°C for 5-6 h in a NMR-tube; monitored by NMR-spectroscopy;
参考文献
Abriel, Walter; Baum, Gerhard; Burdorf, Heike; Heck, Juergen
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1991 , vol. 46, # 7 p. 841 - 852
反应条件
in deuterated toluene
T=0°C; Product distribution;
参考文献
Dehnert, Peter; Grobe, Joseph; Van, Duc Le
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1981 , vol. 36, # 1 p. 48 - 54
反应条件
sodium
1.) liq. NH3, -78 deg, 30 min; Multistep reaction;
参考文献
Kinoshita, Isamu; Kashiwabara, Kazuo; Fujita, Junnosuke; Matsumoto, Keiji; Ooi, Schun'ichiro
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 9 p. 2683 - 2690
反应条件
trimethyltin hydride
T=20 - 60°C; 53 h;
参考文献
Goryunov, Leonid I.; Grobe, Joseph; Shteingarts, Vitalij D.; Krebs, Bernt; Lindemann, Arno; Wuerthwein, Ernst-Ulrich; Mueck-Lichtenfeld, Christian
Chemistry - A European Journal, 2000 , vol. 6, # 24 p. 4612 - 4622
