4-氧代-4-吡啶-3-基丁腈合成路线 （共 8 条）
反应条件
ammonia; hydrogen; nickel in ethanol T=0°C;
参考文献
Mahboobi; Wiegrebe
Archiv der Pharmazie, 1988 , vol. 321, # 3 p. 175 - 177
反应条件
ammonia; hydrogen; nickel in ethanol 40 h; various concentrations and temperatures; Product distribution;
参考文献
Liebigs Annalen der Chemie, , # 2 p. 330 - 333
反应条件
ammonia; hydrogen; nickel in ethanol 40 h; various concentrations and temperatures; Product distribution;
参考文献
Liebigs Annalen der Chemie, , # 2 p. 330 - 333
参考文献
Langhals, Elke; Langhals, Heinz; Ruechardt, Christoph
Liebigs Annalen der Chemie, 1982 , # 5 p. 930 - 949
反应条件
1: 95 percent / Et3N / benzene / 3 h / Heating
2: CH2Cl2 / 1 h / 20 °C
3: 2 N HCl
4: H2O / 40 °C
View Scheme
参考文献
Mahboobi; Wiegrebe
Archiv der Pharmazie, 1988 , vol. 321, # 3 p. 175 - 177
反应条件
1: CH2Cl2 / 1 h / 20 °C
2: 2 N HCl
3: H2O / 40 °C
View Scheme
参考文献
Mahboobi; Wiegrebe
Archiv der Pharmazie, 1988 , vol. 321, # 3 p. 175 - 177
反应条件
in water
T=40°C; Yield given;
参考文献
Mahboobi; Wiegrebe
Archiv der Pharmazie, 1988 , vol. 321, # 3 p. 175 - 177
反应条件
1: 91 percent / conc. H2SO4, FeSO4*7H2O, tButOOH / 1 h / Ambient temperature
2: 65 percent / KOH, 51percent H4N2 / various solvent(s) / 1) 1 h, 110 deg C, 2) heating
View Scheme
参考文献
Langhals, Elke; Langhals, Heinz; Ruechardt, Christoph
Liebigs Annalen der Chemie, 1982 , # 5 p. 930 - 949
