5-(4-甲氧基苯基)-3-苯基-1,2-恶唑合成路线 （共 43 条）
反应条件
[bis(acetoxy)iodo]benzene in neat (no solvent)
参考文献
Chandra Sekhar, Kondapalli Venkata Gowri; Sasank, Thripuraribhatla Venkata Naga Varuna Tara; Nagesh, Hunsur Nagendra; Suresh, Narva; Naidu, Kalaga Mahalakshmi; Suresh, Amaroju
Chinese Chemical Letters, 2013 , vol. 24, # 12 p. 1045 - 1048
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in methanol; water
T=20°C; 7 h; regioselective reaction;
参考文献
Jawalekar, Anup M.; Reubsaet, Erik; Rutjes, Floris P. J. T.; Van Delft, Floris L.
Chemical Communications, 2011 , vol. 47, # 11 p. 3198 - 3200
反应条件
bis-triphenylphosphine-palladium(II) chloride; ammonium hydroxide; hydroxylamine hydrochloride in N,N-dimethyl-formamide
T=20°C; Sonogashira coupling; 37 h;
参考文献
Mohamed Ahmed, Mohamed S.; Kobayashi, Kei; Mori, Atsunori
Organic Letters, 2005 , vol. 7, # 20 p. 4487 - 4489
反应条件
manganese(IV) oxide in benzene
2 h; Heating;
参考文献
Saginova, L. G.; Kukhareva, I. L.; Lebedev, A. T.; Shabarov, Yu. S.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 9.1 p. 1631 - 1638
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 9 p. 1852 - 1860
反应条件
[(2-benzylpyridyl)AuCl2]; silver trifluoromethanesulfonate in methanol; dichloromethane
T=20°C; 2 h;
参考文献
Kung, Karen Ka-Yan; Lo, Vanessa Kar-Yan; Ko, Hok-Ming; Li, Gai-Li; Chan, Pui-Ying; Leung, King-Chi; Zhou, Zhongyuan; Wang, Ming-Zhong; Che, Chi-Ming; Wong, Man-Kin
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2055 - 2070
反应条件
hydroxylamine hydrochloride in ethanol
Heating;
参考文献
Katritzky; Wang; Zhang; Voronkov; Steel
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6787 - 6791
反应条件
chloro(2-dicyclohexylphosphino-2',4',6'-triisoporpyl-1,1'-biphenyl)[2-(2'-amino-1,1'-biphenyl)] palladium (II); copper (II) acetate monohydrate; potassium carbonate in isopropyl alcohol; acetonitrile
T=120°C; Suzuki-Miyaura coupling; 0.333333 h; Microwave irradiation;
参考文献
Grob, Jonathan E.; Nunez, Jill; Dechantsreiter, Michael A.; Hamann, Lawrence G.
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 10241 - 10248
反应条件
1: hydroxylamine hydrochloride; sodium hydroxide / methanol; water / 0.5 h / 20 °C
2: bis-[(trifluoroacetoxy)iodo]benzene / methanol; water / 7 h / 20 °C
View Scheme
参考文献
Jawalekar, Anup M.; Reubsaet, Erik; Rutjes, Floris P. J. T.; Van Delft, Floris L.
Chemical Communications, 2011 , vol. 47, # 11 p. 3198 - 3200
反应条件
1: 64 percent / piperidine / ethanol / 40 h
2: 71 percent / hydroxylamine hydrochloride / ethanol / Heating
View Scheme
参考文献
Katritzky; Wang; Zhang; Voronkov; Steel
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6787 - 6791
反应条件
1: 64 percent / piperidine / ethanol / 40 h
2: 71 percent / hydroxylamine hydrochloride / ethanol / Heating
View Scheme
参考文献
Katritzky; Wang; Zhang; Voronkov; Steel
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6787 - 6791
