反式-环丁烷-1,2-二羰酰氯合成路线 （共 8 条）
反应条件
thionyl chloride in benzene
T=70°C; 24 h;
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: SOCl2 / 7 h / Heating
2: bromine
3: 71 percent / methanol / 56 h / 75 °C
4: aq. HCl / 12 h / Heating
5: 180 °C / water pump
6: 96 percent / SOCl2 / benzene / 24 h / 70 °C
View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: 71 percent / methanol / 56 h / 75 °C
2: aq. HCl / 12 h / Heating
3: 180 °C / water pump
4: 96 percent / SOCl2 / benzene / 24 h / 70 °C
View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: 71 percent / methanol / 56 h / 75 °C
2: aq. HCl / 12 h / Heating
3: 180 °C / water pump
4: 96 percent / SOCl2 / benzene / 24 h / 70 °C
View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: 54 percent / aq. HCl / 144 h / 120 °C
2: 96 percent / SOCl2 / benzene / 24 h / 70 °C
View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: aq. HCl / 12 h / Heating
2: 180 °C / water pump
3: 96 percent / SOCl2 / benzene / 24 h / 70 °C
View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: 180 °C / water pump
2: 96 percent / SOCl2 / benzene / 24 h / 70 °C
View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: bromine
2: 71 percent / methanol / 56 h / 75 °C
3: aq. HCl / 12 h / Heating
4: 180 °C / water pump
5: 96 percent / SOCl2 / benzene / 24 h / 70 °C
View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
