甲基2-乙酰基-2-丙-2-烯基戊-4-烯酸酯合成路线 （共 11 条）
反应条件
sodium hydroxide; tetrabutylammomium bromide in water
参考文献
Nippon Gohsei Kagaku Kogyo Kabushiki Kaisha
Patent: US5101070 A1, 1992 ;
反应条件
triethyl borane; potassium hexamethylsilazane; triphenylphosphine; palladium diacetate in tetrahydrofuran
T=50°C; 1 h;
参考文献
Kimura, Masanari; Mukai, Ryutaro; Tanigawa, Naoko; Tanaka, Shuji; Tamaru, Yoshinao
Tetrahedron, 2003 , vol. 59, # 39 p. 7767 - 7777
反应条件
tetrakis(triphenylphosphine) palladium(0); triphenylphosphine in tetrahydrofuran
7 h;
参考文献
Lu, Xiyan; Jiang, Xiaohui; Tao, Xiaochun
Journal of Organometallic Chemistry, 1988 , vol. 344, p. 109 - 118
反应条件
(pentamethylcyclopentadienyl)Ru(1,5-cyclooctadiene)Cl in 1,2-dichloro-ethane
T=90°C; 5 h;
参考文献
Yamamoto, Yoshihiko; Nakagai, Yu-Ichiro; Itoh, Kenji
Chemistry - A European Journal, 2004 , vol. 10, # 1 p. 231 - 236
反应条件
tetrakis(triphenylphosphine) palladium(0); triphenylphosphine in tetrahydrofuran
T=65°C; 7 h; Yield given. Yields of byproduct given;
参考文献
Lu, Xiyan; Jiang, Xiaohui; Tao, Xiaochun
Journal of Organometallic Chemistry, 1988 , vol. 344, p. 109 - 118
反应条件
sodium hydride in N,N-dimethyl-formamide; mineral oil
T=0 - 20°C; Inert atmosphere;
参考文献
Aissa, Christophe; Ho, Kelvin Y. T.; Tetlow, Daniel J.; Pin-No, Maria
Angewandte Chemie - International Edition, 2014 , vol. 53, # 16 p. 4209 - 4212
Angew. Chem., 2014 , vol. 126, # 16 p. 4293 - 4296,4
反应条件
Ni(1,4-bis(diphenylphosphanyl)butane)2 in N,N-dimethyl-formamide
T=80°C; 0.1 h; other catalysts, solvents and times; Product distribution;
参考文献
Bricout, Herve; Carpentier, Jean-Francois; Mortreux, Andre
Chemical Communications, 1997 , # 15 p. 1393 - 1394
反应条件
phenolated sodium; palladium
参考文献
Takahashi,K. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 230 - 236
反应条件
1-methyl-piperidine; [Ru(η4-C8H12)(η6-C8H10)]
T=50°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zhang, Shi-Wei; Mitsudo, Take-aki; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1993 , vol. 450, # 1.2 p. 197 - 207
反应条件
polypyrrole supported phosphine borane complex (6.4 molpercent); sodium hydride; palladium diacetate in tetrahydrofuran
48 h; Ambient temperaturevarious borane complexes; Product distribution;
参考文献
Riegel, Nadege; Darcel, Christophe; Stephan, Olivier; Juge, Sylvain
Journal of Organometallic Chemistry, 1998 , vol. 567, # 1-2 p. 219 - 233
