1: pyridine / 72 h / Ambient temperature
2: KOH / methanol / 1.) room temperature, 14 h, 2.) reflux, 1 h
3: NCS / CCl4 / 14 h / Ambient temperature
4: TFA / 1 h / -6 °C
5: NaIO4 / methanol; H2O / Ambient temperature
6: 0.5 h / 130 °C / 20 Torr
View Scheme
参考文献
Harvey, Jeremy; Brichard, Marie-Helene; Viehe, Heinz G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 19 p. 2275 - 2280
1: KOH / methanol / 1.) room temperature, 14 h, 2.) reflux, 1 h
2: NCS / CCl4 / 14 h / Ambient temperature
3: TFA / 1 h / -6 °C
4: NaIO4 / methanol; H2O / Ambient temperature
5: 0.5 h / 130 °C / 20 Torr
View Scheme
参考文献
Harvey, Jeremy; Brichard, Marie-Helene; Viehe, Heinz G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 19 p. 2275 - 2280
1: NaIO4 / methanol; H2O / Ambient temperature
2: 0.5 h / 130 °C / 20 Torr
View Scheme
参考文献
Harvey, Jeremy; Brichard, Marie-Helene; Viehe, Heinz G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 19 p. 2275 - 2280
1: NCS / CCl4 / 14 h / Ambient temperature
2: TFA / 1 h / -6 °C
3: NaIO4 / methanol; H2O / Ambient temperature
4: 0.5 h / 130 °C / 20 Torr
View Scheme
参考文献
Harvey, Jeremy; Brichard, Marie-Helene; Viehe, Heinz G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 19 p. 2275 - 2280
1: TFA / 1 h / -6 °C
2: NaIO4 / methanol; H2O / Ambient temperature
3: 0.5 h / 130 °C / 20 Torr
View Scheme
参考文献
Harvey, Jeremy; Brichard, Marie-Helene; Viehe, Heinz G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 19 p. 2275 - 2280
