1,4-苯并二噁烷-2-羧酸甲酯合成路线 （共 17 条）
反应条件
water; lithium hydroxide hydrate in tetrahydrofuran 3 h;
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
反应条件
water; lithium hydroxide hydrate in tetrahydrofuran 3 h;
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
反应条件
1: whole cells of Arthrobacter sp. ABL MTCC No. 5125 lipase / aq. phosphate buffer; di-isopropyl ether / 2 h / 25 °C / pH 7.1 2: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / |Inert atmosphere View Scheme
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
反应条件
1: titanium tetrachloride; sodium tetrahydroborate / ethylene glycol dimethyl ether / 0 - 20 °C
2: pyridine / 0 - 20 °C
View Scheme
参考文献
Liu, Xin; Wang, Songlin; Chen, Yin; Liu, Xinghua; Xu, Xiangqing; Liu, Bi-Feng; Zhang, Guisen
Archiv der Pharmazie, 2014 , vol. 347, # 1 p. 32 - 41
反应条件
1: titanium tetrachloride; sodium tetrahydroborate / ethylene glycol dimethyl ether / 0 - 20 °C
2: pyridine / 0 - 20 °C
3: ethanol / |Reflux
View Scheme
参考文献
Liu, Xin; Wang, Songlin; Chen, Yin; Liu, Xinghua; Xu, Xiangqing; Liu, Bi-Feng; Zhang, Guisen
Archiv der Pharmazie, 2014 , vol. 347, # 1 p. 32 - 41
反应条件
1: whole cells of Arthrobacter sp. ABL MTCC No. 5125 lipase / aq. phosphate buffer; di-isopropyl ether / 2 h / 25 °C / pH 7.1
2: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran; dichloromethane / 0.17 h / 0 °C
3: trifluoroacetic acid / dichloromethane / 1 h / 0 °C
View Scheme
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
反应条件
1: whole cells of Arthrobacter sp. ABL MTCC No. 5125 lipase / aq. phosphate buffer; di-isopropyl ether / 2 h / 25 °C / pH 7.1
2: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran; dichloromethane / 0.17 h / 0 °C
3: trifluoroacetic acid / dichloromethane / 1 h / 0 °C
View Scheme
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
