1,4-苯并二噁烷-2-羧酸甲酯合成路线 （共 17 条）
反应条件
potassium carbonate in acetone 18 h; Reflux;
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
反应条件
sulfuric acid 1 h; Heating;
参考文献
Tomiyama; Wakabayashi; Yokota
Journal of Medicinal Chemistry, 1989 , vol. 32, # 8 p. 1988 - 1996
反应条件
1: 98 percent / HOAc, conc. H2SO4 / H2O / 15 h / 110 °C 2: 97 percent / conc. H2SO4 / 1 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 32, # 8 p. 1988 - 1996
反应条件
1: 85 percent / K2CO3 / acetone / 12 h / Heating 2: 98 percent / HOAc, conc. H2SO4 / H2O / 15 h / 110 °C 3: 97 percent / conc. H2SO4 / 1 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 32, # 8 p. 1988 - 1996
参考文献
Gazzetta Chimica Italiana, , vol. 88, p. 214,215
反应条件
sodium tetrahydroborate; titanium tetrachloride in ethylene glycol dimethyl ether T=0 - 20°C;
参考文献
Archiv der Pharmazie, , vol. 347, # 1 p. 32 - 41
反应条件
1: lithium hydroxide hydrate; water / tetrahydrofuran / 4 h / 20 °C 2: thionyl chloride / 1 h / |Reflux View Scheme
参考文献
Wang, Songlin; Chen, Yin; Zhao, Song; Xu, Xiangqing; Liu, Xin; Liu, Bi-Feng; Zhang, Guisen
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 7 p. 1766 - 1770
反应条件
water; lithium hydroxide hydrate in tetrahydrofuran 3 h;
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
反应条件
water; lithium hydroxide hydrate in tetrahydrofuran 3 h;
参考文献
Tetrahedron Asymmetry, , vol. 23, # 22-23 p. 1615 - 1623
反应条件
1: whole cells of Arthrobacter sp. ABL MTCC No. 5125 lipase / aq. phosphate buffer; di-isopropyl ether / 2 h / 25 °C / pH 7.1 2: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / |Inert atmosphere View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 23, # 22-23 p. 1615 - 1623
