N-(4-氟苯基)苯甲酰胺合成路线 （共 29 条）
反应条件
zinc(II) chloride anschliessend Erhitzen mit wss. H2SO4;
参考文献
Journal of the Chemical Society, , p. 2205,2207, 2209
反应条件
1: Lawesson's reagent 2: sodium hydroxide; potassium hexacyanoferrate(III) / ethanol; water / 3.08 h / 80 - 90 °C View Scheme
参考文献
Escudero, Daniel; Heuser, Eike; Meier, Robert J.; Schaeferling, Michael; Thiel, Walter; Holder, Elisabeth
Chemistry - A European Journal, 2013 , vol. 19, # 46 p. 15639 - 15644
反应条件
copper(l) iodide; manganese(II) fluoride; rel-(R,R)-DACH; potassium hydroxide in water
T=60°C; 24 h;
参考文献
Teo, Yong-Chua; Yong, Fui-Fong; Ithnin, Idzham Khalid; Yio, Siew-Hui Trionna; Lin, Zhiyin
European Journal of Organic Chemistry, 2013 , # 3 p. 515 - 524
反应条件
copper(l) iodide; acetaldehyde oxime; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=120°C; 15 h; Inert atmosphereSchlenk technique;
参考文献
Zhang, Dong-Xue; Xiang, Shi-Kai; Hu, Hao; Tan, Wen; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Tetrahedron, 2013 , vol. 69, # 47 p. 10022 - 10029
反应条件
triethylamine in ethyl acetate
T=0 - 20°C; 4 h;
参考文献
Ueda, Satoshi; Nagasawa, Hideko
Journal of Organic Chemistry, 2009 , vol. 74, # 11 p. 4272 - 4277
反应条件
triethylamine in tetrahydrofuran
T=20°C; 2 h;
参考文献
ASTEX THERAPEUTICS LIMITED
Patent: WO2006/70198 A1, 2006 ;
Location in patent: Page/Page column 171-172 ;
WO 2006/070198 A1
反应条件
titanium tetra-n-butoxide in o-xylene
T=145°C; 2 h;
参考文献
Shteinberg, L. Ya.; Kondratov, S. A.; Shein, S. M.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 9.2 p. 1758 - 1762
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 9 p. 1945 - 1949
反应条件
1,10-phenanthroline; oxygen; copper(II) bis(trifluoromethanesulfonate); potassium carbonate in dimethyl sulfoxide
T=140°C; 72 h; Schlenk technique;
参考文献
Xu, Mei; Zhang, Xiao-Hong; Shao, Yin-Lin; Han, Jiang-Sheng; Zhong, Ping
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2665 - 2670,6
Title/Abstract Full Text Show Details
Xu, Mei; Zhang, Xiao-Hong; Shao, Yin-Lin; Han, Jiang-Sheng; Zhong, Ping
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2665 - 2670
反应条件
1: 4-fluoroaniline With C63H108Cl3Li3N9NdO9 in tetrahydrofuran
0.5 h; Inert atmosphere;
2: benzaldehyde in tetrahydrofuran
T=25°C; 3 h; Inert atmosphere;
参考文献
Qian, Cunwei; Zhang, Xingmin; Zhang, Yong; Shen, Qi
Journal of Organometallic Chemistry, 2010 , vol. 695, # 5 p. 747 - 752
反应条件
di-tert-butyl peroxide; potassium hydroxide in chlorobenzene
T=140°C; 24 h;
参考文献
Xiao, Fuhong; Liu, Yong; Tang, Chenglin; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 4 p. 984 - 987
