4-甲基-5-吡啶-4-基-4H-[1,2,4]三唑-3-硫醇合成路线 (共 5 条)
反应条件
sodium hydroxide 0.5 h; Heating;
参考文献
Brown; Cowden
Australian Journal of Chemistry, 1983 , vol. 36, # 7 p. 1469 - 1475
反应条件
1: With pyridine T=20°C; 2: With sodium hydroxide; water T=60°C; 16 h;
参考文献
ASTRAZENECA AB; NPS PHARMACEUTICALS, INC.
Patent: WO2005/80356 A1, 2005 ;
Location in patent: Page/Page column 57 ;
WO 2005/080356 A1
反应条件
1: 95 percent / ethanol / 0.42 h / Heating 2: 78 percent / 1M aq. NaOH / 0.5 h / Heating View Scheme
参考文献
Australian Journal of Chemistry, , vol. 36, # 7 p. 1469 - 1475
反应条件
sodium hydroxide in ethanol
T=20°C;
参考文献
ASTRAZENECA AB; NPS PHARMACEUTICALS, INC.
Patent: WO2005/80379 A1, 2005 ;
Location in patent: Page/Page column 40 ;
WO 2005/080379 A1