2,2-二氟-1,3-二苯基-1,3-丙二酮合成路线 （共 7 条）
反应条件
Fluolead; Olah's reagent in dichloromethane T=20°C; 24 h; Inert atmosphere;
参考文献
Umemoto, Teruo; Singh, Rajendra P.; Xu, Yong; Saito, Norimichi
Journal of the American Chemical Society, 2010 , vol. 132, # 51 p. 18199 - 18205
反应条件
1-Fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; zinc(II) chloride in 1,2-dichloro-ethane
T=60°C; 18 h;
参考文献
Umemoto, Teruo; Fukami, Shinji; Tomizawa, Ginjiro; Harasawa, Kikuko; Kawada, Kosuke; Tomita, Kyoichi
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8563 - 8575
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile
T=82°C; 0.166667 h; microwave irradiation;
参考文献
Xiao, Ji-Chang; Shreeve, Jean'ne M.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 4 p. 475 - 478
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); triethylamine in acetonitrile
T=-10°C; 0.5 h;
参考文献
Peng, Weimin; Shreeve, Jean'ne M.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5760 - 5763
反应条件
XeF2; potassium hydrogen difluoride in dichloromethane
Ambient temperature;
参考文献
Stavber, Stojan; Sket, Boris; Zajc, Barbara; Zupan, Marko
Tetrahedron, 1989 , vol. 45, # 18 p. 6003 - 6010
反应条件
XeF2; potassium hydrogen difluoride in dichloromethane
Ambient temperature;
参考文献
Stavber, Stojan; Sket, Boris; Zajc, Barbara; Zupan, Marko
Tetrahedron, 1989 , vol. 45, # 18 p. 6003 - 6010
反应条件
aluminium trichloride
参考文献
Fear et al.
Journal of the Chemical Society, 1956 , p. 3199,3202
