1-(十二基氧基)-4-((4-乙炔苯基)乙炔)苯合成路线 （共 4 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-78 - 0°C; 3 h;
参考文献
Armaroli, Nicola; Accorsi, Gianluca; Rio, Yannick; Ceroni, Paola; Vicinelli, Veronica; Welter, Richard; Gu, Tao; Saddik, Mohamed; Holler, Michel; Nierengarten, Jean-Francois
New Journal of Chemistry, 2004 , vol. 28, # 12 p. 1627 - 1637
反应条件
1.1: Zn; PPh3 / CH2Cl2 / 24 h / 20 °C 1.2: 95 percent / CH2Cl2 / 0 - 20 °C 2.1: 86 percent / LDA / tetrahydrofuran / 3 h / -78 - 0 °C View Scheme
参考文献
Armaroli, Nicola; Accorsi, Gianluca; Rio, Yannick; Ceroni, Paola; Vicinelli, Veronica; Welter, Richard; Gu, Tao; Saddik, Mohamed; Holler, Michel; Nierengarten, Jean-Francois
New Journal of Chemistry, 2004 , vol. 28, # 12 p. 1627 - 1637
反应条件
1.1: 70 percent / CuI; PdCl2(PPh3)2; Et3N / 48 h / 20 °C 2.1: Zn; PPh3 / CH2Cl2 / 24 h / 20 °C 2.2: 95 percent / CH2Cl2 / 0 - 20 °C 3.1: 86 percent / LDA / tetrahydrofuran / 3 h / -78 - 0 °C View Scheme
参考文献
Armaroli, Nicola; Accorsi, Gianluca; Rio, Yannick; Ceroni, Paola; Vicinelli, Veronica; Welter, Richard; Gu, Tao; Saddik, Mohamed; Holler, Michel; Nierengarten, Jean-Francois
New Journal of Chemistry, 2004 , vol. 28, # 12 p. 1627 - 1637
反应条件
1.1: 70 percent / CuI; PdCl2(PPh3)2; Et3N / 48 h / 20 °C 2.1: Zn; PPh3 / CH2Cl2 / 24 h / 20 °C 2.2: 95 percent / CH2Cl2 / 0 - 20 °C 3.1: 86 percent / LDA / tetrahydrofuran / 3 h / -78 - 0 °C View Scheme
参考文献
Armaroli, Nicola; Accorsi, Gianluca; Rio, Yannick; Ceroni, Paola; Vicinelli, Veronica; Welter, Richard; Gu, Tao; Saddik, Mohamed; Holler, Michel; Nierengarten, Jean-Francois
New Journal of Chemistry, 2004 , vol. 28, # 12 p. 1627 - 1637
