DL-3-氨基-3-苯基丙酸合成路线 （共 124 条）
反应条件
hydroxylamine hydrochloride; sodium ethanolate in ethanol 9 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 59, # 24 p. 7292 - 7298
反应条件
naphthalene; sodium in ethylene glycol dimethyl ether Yield given;
参考文献
Tetrahedron, , vol. 49, # 48 p. 11329 - 11340
反应条件
hydrogenchloride T=25°C; 24 h;
参考文献
Tetrahedron, , vol. 50, # 27 p. 8099 - 8102
反应条件
hydrogenchloride in 1,4-dioxane 0.75 h; Ambient temperature;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 6, # 10 p. 1707 - 1730
反应条件
1.1: n-BuLi; diisopropylamine / tetrahydrofuran; hexane / 2 h / -78 °C 1.2: 82 percent / Na; i-PrOH / tetrahydrofuran; hexane / 20 °C 2.1: 90 percent / aq. HCl / Heating View Scheme
参考文献
Tetrahedron, , vol. 57, # 4 p. 703 - 712
反应条件
1: 95 percent / Na; isopropanol / tetrahydrofuran / 0 - 20 °C 2: 90 percent / aq. HCl / Heating View Scheme
参考文献
Tetrahedron, , vol. 57, # 4 p. 703 - 712
反应条件
1: K2CO3 / methanol; H2O 2: aq. HCl / dioxane / 0.75 h / Ambient temperature View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 6, # 10 p. 1707 - 1730
反应条件
1: 95 percent / pyridinium chlorochromate / CH2Cl2 / 24 h / 25 °C 2: 78 percent / NH2OH*H2O, pyridine / ethanol / 1 h / Heating 3: 74 percent / LiAlH4 / tetrahydrofuran / 8 h / 80 - 85 °C 4: 5N HCl / 24 h / 25 °C View Scheme
参考文献
Tetrahedron, , vol. 50, # 27 p. 8099 - 8102
反应条件
1: 78 percent / NH2OH*H2O, pyridine / ethanol / 1 h / Heating 2: 74 percent / LiAlH4 / tetrahydrofuran / 8 h / 80 - 85 °C 3: 5N HCl / 24 h / 25 °C View Scheme
参考文献
Tetrahedron, , vol. 50, # 27 p. 8099 - 8102
