2-(苯基甲基)萘-1-醇合成路线 (共 13 条)
反应条件
in neat (no solvent) T=125°C; 1 h; Microwave irradiation;
参考文献
Balint, Erika; Kovacs, Orsolya; Drahos, Laszlo; Keglevich, Gyoergy
Letters in Organic Chemistry, 2013 , vol. 10, # 5 p. 330 - 336
反应条件
T=22°C; Solid phase reaction; photo-Fries reaction; 0.25 h; Photolysis; Product distributionKinetics; Further Variations:polyolefin film type;
参考文献
Gu, Weiqiang; Warrier, Manoj; Ramamurthy; Weiss, Richard G.
Journal of the American Chemical Society, 1999 , vol. 121, # 40 p. 9467 - 9468
反应条件
1: 55 percent / isoamyl nitrite / CH2Cl2; tetrahydrofuran / 1.5 h / Heating 2: conc. HCl / methanol / 16 h / Heating View Scheme
参考文献
Batt, Douglas G.; Jones, David G.; Greca, Susan La
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6704 - 6708
反应条件
1: 70 percent / LiAlH4, AlCl3 / diethyl ether / 1 h / Ambient temperature 2: 55 percent / isoamyl nitrite / CH2Cl2; tetrahydrofuran / 1.5 h / Heating 3: conc. HCl / methanol / 16 h / Heating View Scheme
参考文献
Batt, Douglas G.; Jones, David G.; Greca, Susan La
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6704 - 6708
反应条件
in tert-butyl alcohol other aldehydes, other tetralones; Product distribution;
参考文献
Batt; Maynard; Petraitis; Shaw; Galbraith; Harris
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 360 - 370
反应条件
hydrogenchloride in methanol 16 h; Heating; Yield given. Yields of byproduct given;
参考文献
Batt, Douglas G.; Jones, David G.; Greca, Susan La
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6704 - 6708
反应条件
palladium on activated charcoal T=240°C;
参考文献
Campbell et al.
Pr. roy. Soc. Edinburgh, 1957 , vol. <A> 65, p. 223,225
反应条件
mercury; zinc Reduction;
参考文献
Gu, Weiqiang; Weiss, Richard G.
Tetrahedron, 2000 , vol. 56, # 36 p. 6913 - 6925
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1925 , vol. 442, p. 243
Angewandte Chemie, 1923 , vol. 36, p. 478
Full Text Show Details
Claisen
Patent: DE412169 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 15, p. 267
反应条件
in hexane Irradiation; Further byproducts. Title compound not separated from byproducts.;
参考文献
Kaanumalle, Lakshmi S.; Gibb, Corinne L. D.; Gibb, Bruce C.; Ramamurthy
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 2 p. 236 - 238